Universal quantitative NMR analysis of complex natural samples

Quantitative analysis of phospholipids by 31P-NMR.

High-field 31P nuclear magnetic resonance spectroscopy was used to quantitate phospholipids in mixtures in organic solvents. The sample is dissolved in chloroform-methanol and analyzed at 161.7 MHz with decoupling of the protons. Signals were identified using authentic compounds, and their relative distribution was measured in mole percent. The method has good accuracy and reproducibility, and ...

NMR-Spectroscopy in Drug Analysis Quantitative NMR Spectroscopy

Application of the Ratio Derivative Method in Quantitative Analysis of Samples Dyed with Ternary Dye Mixtures

In this study, a derivative method is applied for the determination of dye concentration in fabrics dyed with tricomponent dye mixtures. The reflectance of spectra of the samples were recorded between 400 and 700 nm. Initially, the obtained (K/S) spectra were divided by the spectrum of a standard sample dyed with two of the components in the ternary mixture and the derivative spectra were calcu...

Improved method for isotopic and quantitative analysis of dissolved inorganic carbon in natural water samples.

We present here an improved and reliable method for measuring the concentration of dissolved inorganic carbon (DIC) and its isotope composition (delta(13)C(DIC)) in natural water samples. Our apparatus, a gas chromatograph coupled to an isotope ratio mass spectrometer (GCIRMS), runs in a quasi-automated mode and is able to analyze about 50 water samples per day. The whole procedure (sample prep...

Natural and Anthropogenic Source of Heavy Metals Pollution in the Soil Samples of an Industrial Complex a Case Study

Background: Soil serves as a major reservoir for contaminants as it can bind to various chemicals. The aim of this study was to evaluate the levels of some metals (Cd, Cu, Fe and V) in soil samples collected from different stations of Ahvaz Industrial Complex II to determine the natural and anthropogenic contribution of metal in the soil. Methods: This was an experimental study that carried ou...